Static Headspace-Gas Chromatography Theory and Practice - used book

EAN (ISBN-13): 9780471749448
ISBN (ISBN-10): 0471749443
Hardcover
Publishing year: 2006
Publisher: Wiley-Interscience
349 Pages
Weight: 0,635 kg
Language: eng/Englisch

Book in our database since 2007-05-29T11:02:35+01:00 (London)
Detail page last modified on 2023-11-30T10:33:37+00:00 (London)
ISBN/EAN: 9780471749448

ISBN - alternate spelling:
0-471-74944-3, 978-0-471-74944-8
Alternate spelling and related search-keywords:
Book author: kolb, bruno, ettre, leslie
Book title: rom, static, chromatography, sorry out gas, headspace, theory wants, the practice

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Information from Publisher

Author: Bruno Kolb; Leslie S. Ettre
Title: Static Headspace-Gas Chromatography - Theory and Practice
Publisher: Wiley-Interscience; John Wiley & Sons
376 Pages
Publishing year: 2006-06-13
Weight: 0,630 kg
Language: English
162,00 € (DE)
Not available (reason unspecified)
160mm x 238mm x 22mm

BB; Hardcover, Softcover / Chemie; Chromatographie; Chemie; Chemistry; Chromatographie / Trennverfahren; Chromatography / Separation Techniques; Gaschromatographie; Chromatographie / Trennverfahren

Preface. Preface to the First Edition. List of Acronyms and Symbols. 1. General introduction. 1.1 Principles of headspace analysis . 1.2 Types of headspace analysis. 1.3 The evolution of the HS-GC methods. 1.4 Headspace -- gas chromatography literature. 1.5 Regulatory methods utilizing (static) HS-GC. 1.6 References. 2. Theoretical background of HS-GC and its applications. 2.1 Basic theory of headspace analysis. 2.2 Basic physicochemical relationships. 2.3 Headspace sensitivity. 2.4 Headspace linearity. 2.5 Duplicate analyses. 2.6 Multiple headspace extraction (MHE). 2.7 References. 3. The technique of HS-GC. 3.1 Sample vials. 3.2 Caps. 3.3 Septa. 3.4 Thermostatting. 3.5 The fundamentals of headspace sampling systems. 3.6 Use of open-tubular (capillary) columns. 3.7 Enrichment techniques in HS-GC. 3.8 Special techniques with the balanced-pressure systems. 3.9. Reaction HS-GC. 3.10 References. 4. Sample handling in HS-GC. 4.1 Equilibration. 4.2 Solution approach. 4.3 Sample handling and sample introduction. 4.4 Preparation of standard solutions. 4.5 Influence of the matrix. 4.6 Methods aiming the complete evaporation of the analyte. 4.7 References. 5. Headspace methods for quantitative analysis. 5.1 Internal normalization. 5.2 Internal standard method. 5.3 External standard method. 5.4 Standard addition method. 5.5 Multiple headspace extraction (MHE). 5.6 Analysis of solid samples (adsorption systems). 5.7 Calibration techniques with headspace samples of varying volumes. 5.8 Analysis of gas samples. 5.9 References. 6. Method development in HS-GC. 6.1 General guidelines. 6.2 Determination of the residual monomer content of polystyrene pellets. 6.3 Determination of residual solvents in a printed plastic film. 6.4 Determination of the volatile constituents of a cathodic electrolytic plating bath. 7. Nonequilibrium static headspace analysis. 7.1 Accelerated analysis. 7.2 Heat-sensitive samples. 7.3 References. 8. Qualitative analysis by HS-GC. 8.1 The use of HS-GC in 'fingerprinting.'. 8.2 The use of headspace sampling in hyphenated systems. 8.3 The use of HS-GC in microbiology. 8.4 References. 9. Special measurements. 9.1 Determination of vapor pressures. 9.2 Determination of activity coefficients. 9.3 Determination of related physicochemical functions. 9.4 Determination of phase distribution (partition coefficient). 9.5 Reaction constant measurements. 9.6 Determination of solute solubility by MHE. 9.7 Gas-solid systems. 9.8 Validation of the headspace instrumentation: investigation of detector linearity and detection limit. 9.9 References. Index.